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SLUDGE

No Komoditi Parameter Metoda
E SLUDGE   PP NO. 85 / 1999
    Uji Karakterisasi Pendahuluan Limbah B3  
    Screening of Lazardous Waste :  
    *) + Radioactive  
    *) non Radioactive  
       
    Uji TCLP  
    *) Preparasi dan Analisa Anorganik US EPA SW 846 method 1311
    *) Preparasi dan Analisa Organik US EPA SW 846 method 1311
    Uji Toksisitas Akut LD-50 ASTM Designation E 1163-90

 SLUDGE (DRY BASIC)

   
   
   
er  Metode 
   
Characteristric test  ASTM 
Screening of Lazardous Waste :  ASTM 
a. + Radioactive  
b. Non Radioactive  
TCLP test  US EPA SW 846 Method 1311 
(Toxicity Characteristic Leaching Procedure) :  
A.  Inorganic Analysis  
- Arsenic   US EPA SW-846-7061A 
- Barium  US EPA SW-846-6010B 
- Boron  US EPA SW-846-6010B 
- Cadmium  US EPA SW-846-6010B 
- Chromium  US EPA SW-846-6010B 
- Copper  US EPA SW-846-6010B 
- Free Cyanide  US EPA 335.2 
- Fluoride  4500-F-D * 
- Lead  US EPA SW-846-6010B 
- Mercury  US EPA SW-846-7470 
- Nitrate + Nitrite  4500-NO3-F / 4500-NO2-B * 
- Nitrite  4500-NO2-B * 
- Selenium  US EPA SW-846-7741 
- Silver  US EPA SW-846-6010B 
- Zinc  US EPA SW-846-6010B 
- Antimoni  
- Berilium  
- Chromium 6+  
- Molibdenum  
- Tributil Tin Oxide  
- Klorida  
- Iodida  
   
   
B. Organic Analysis  
- Aldrine + Dieldrine  US EPA SW-846-8081A 
- Benzene  US EPA SW-846-5030 
- Carbon Tetrachloride  US EPA SW-846-5030 
- Chlordane  US EPA SW-846-8081A 
- Chlorobenzene  US EPA SW-846-8020 
- Chloroform  US EPA SW 846-5030 
- o-Cresol  US EPA SW 846-8270C 
- m-Cresol  US EPA SW 846-8270C 
- p-Cresol  US EPA SW 846-8270C 
- Total Cresol  US EPA SW 846-8270C 
- 2,4-D  US EPA SW 846-8150 
- 1,4 Dichlorobenzene  US EPA SW 846-8270C 
- 1,2 Dichloroethane  US EPA SW 846-5030 
- 1,1 Dichloroethylene  US EPA SW 846-5030 
- 2,4 Dinitrotoluene  US EPA SW 846-8270C 
- Endrin  US EPA SW-846-8081A 
- Heptachlor + H. Epoxide  US EPA SW-846-8081A 
- Hexachlorobenzene  US EPA SW 846-8270C 
- Hexachlorobutadiene  US EPA SW 846-8270C 
- Hexachloroethane  US EPA SW 846-8270C 
- Lindane  US EPA SW-846-8081A 
- Metoxychlor  US EPA SW-846-8081A 
- Methyl Ethyl Kethon  US EPA SW-846-5030 
- Methyl Parathion  US EPA SW-846-8080 
- Nitrobenzene  US EPA SW 846-8270C 
- Nitriloatriacetic Acid  US EPA SW-846-5030 
- Pentachlorophenol  US EPA SW 846-8270C 
- Pyridine  US EPA SW 846-8270C 
- Parathion  US EPA SW-846-8080 
- PCBs  US EPA SW-846-8082 
- Tetrachloroethylene  US EPA SW-846-5030 
- Toxaphene  US EPA SW-846-8081A 
- Trichloroethylene  US EPA SW-846-5030 
- Trihalomethane  US EPA SW-846-5030 
- 2,4,5 Trichlorophenol  US EPA SW 846-8270C 
- 2,4,6 Trichlorophenol  US EPA SW 846-8270C 
- 2,4,5-TP (Silvex)  US EPA SW-846-8040 
- Vinyl Chloride  US EPA SW-846-5030 
   
DDT+DDD+DDE  
-2-Chlorofenol  
Di(2-Ethylheksil) ftalat  
Dichloromethane  
2,4-dichlorofenol  
Ethylbenzene  
EDTA  
Formaldehide  
Fenol (total)  
Styrene  
1,1,1,2-tetrachloroethane  
1,1,2,2-tetrachloroethane  
toluene  
trichlorobenzene (total)  
1,1,1-trichloroethane  
1,1,2-trichloroethane  
   
   
   
   
   
   
   
C. Acute Toxicity Test LD-50  ASTM E 1163-98/US EPA 
   
D. Toxicity Test LC-50   US EPA 5th Ed, 2002  (water) / ASTM E 1163-90/ 
-  Cyprinus carpio ( ikan mas )  US EPA 40 CFR Ch 1 PART 435 (drilling fluids) 
-  P. monodon ( udang )  
   
 Total Konsentrasi   
A. Base metal (solid, water and oil )  
a. Preparation  US EPA SW-846-3050B 
b. Analysis  :  
- Silver  US EPA SW-846-6010B 
- Alumunium (Al)  US EPA SW-846-6010B 
- Barium (Ba)  US EPA SW-846-6010B 
- Boron (B)  US EPA SW-846-6010B 
- Calcium (Ca)  US EPA SW-846-6010B 
- Cadmium (Cd)  US EPA SW-846-6010B 
- Cobalt (Co)  US EPA SW-846-6010B 
- Chromium (Cr)  US EPA SW-846-6010B 
- Copper (Cu)  US EPA SW-846-6010B 
- Iron (Fe)  US EPA SW-846-6010B 
- Potasium (K)  US EPA SW-846-6010B 
- Magnesium (Mg)  US EPA SW-846-6010B 
- Molybdenum (Mo)  US EPA SW-846-6010B 
- Mangan (Mn)  US EPA SW-846-6010B 
- Sodium (Na)  US EPA SW-846-6010B 
- Nickel (Ni)  US EPA SW-846-6010B 
- Lead (Pb)  US EPA SW-846-6010B 
- Stanum (Sn)  US EPA SW-846-6010B 
- Zinc (Zn)  US EPA SW-846-6010B 
   
B. Hydride (sludge,water and  oil)  
a. Preparasi  US EPA SW-846-3050 
b. Analisa  
- Arsenic  US EPA SW-846-7061 
- Selenium (Se)  US EPA SW-846-7741 
   
C. Mercury (Hg) (sludge,water and oil)  US EPA SW-846-7471A 
   
D. Anion (sludge,water and oil)  
- Fluorida  US EPA Method 340.1 
- Chloride  4500-CI-D 
- Nitrate / Nitrite  133A*/4500-NO2-F 
- Phenol  US EPA Method 420.1 
- Ammonium  US EPA Method 350.2 
- Sulphide  US EPA Method 376.2 
- Cyanide  US EPA Method 335.3 
- Sulphate  US EPA Method 375.4 
   
E. Volatile Organic  untuk contoh Padat/ Sludge 
- Benzene  US EPA SW-846-5030 
- Methyl Ethyl Kethon (MEK)  US EPA SW-846-5030 
- Chlorobenzene  US EPA SW-846-5030 
- Vynil chloride monomer  US EPA SW-846-5030 
- Trihalomethane  US EPA SW-846-5030 
- CCl4  US EPA SW-846-5030 
- 1,4-Dichlorobenzene  US EPA SW-846-5030 
- 1,2-Dichloroethane  US EPA SW-846-5030 
- 1,1-Dichloroethylene  US EPA SW-846-5030 
- Trichloroethylene   US EPA SW-846-5030 
- Tetrachloroethylene  US EPA SW-846-5030 
- 1,1,1-Trichloroethane  US EPA SW-846-5030 
   
F. Non-volatile organic  untuk contoh Padat/ Sludge 
a. Organochlorine  
- Aldrine  US EPA SW-846-3540 A,3620 A  & 8081A 
- Dieldrine  US EPA SW-846-3540 A,3620 A  & 8081A 
- Chlordane  US EPA SW-846-3540 A,3620 A  & 8081A 
- Endrine  US EPA SW-846-3540 A,3620 A  & 8081A 
- Heptachlor   US EPA SW-846-3540 A,3620 A  & 8081A 
- Heptachlor epoxide  US EPA SW-846-3540 A,3620 A  & 8081A 
- Hexachloroethane  US EPA SW-846-3540 A,3620 A  & 8270C 
- Parathion  US EPA SW-846-3540 A,3620 A  & 8080 
- Methyl Parathion  US EPA SW-846-3540 A,3620 A  & 8080 
- Toxaphene  US EPA SW-846-3540 A,3620 A  & 8080 
- 2,4,5-TP (Silvex)  US EPA SW-846-3540 A,3620 A  & 8080 
- 2,4-D   US EPA SW-846-3540 A,3620 A  & 8080 
- Methoxychlor  US EPA SW-846-3540 A,3620 A  & 8080 
   
b. 2,4-D   US EPA SW-846-3540 A,3620 A  & 8080 
   
c. PCBs  (soil)  US EPA SW-846-3540 A,3620 A & 8082 
   
d. Phenol Group  
- o-Cresol  US EPA SW-846-3540 A,3620 A  & 8270C 
- m-Cresol  US EPA SW-846-3540 A,3620 A  & 8270C 
- p-Cresol  US EPA SW-846-3540 A,3620 A  & 8270C 
- PCP  US EPA SW-846-3540 A,3620 A  & 8270C 
- 2,4,5-Trichlorophenol  US EPA SW-846-3540 A,3620 A  & 8270C 
- 2,4,6-Trichlorophenol  US EPA SW-846-3540 A,3620 A  & 8270C 
   
e. 2,4-Dinitrotoluene, Nitrobenzene, Pyridine  
- 2,4-Dinitrotoluene  US EPA SW-846-3540 A,3620 A  & 8080 
- Nitrobenzene  US EPA SW-846-3540 A,3620 A & 8080 
- Pyridine  US EPA SW-846-3540 A,3620 A & 8080 
   
f. Nitrotriacetic acid  US EPA SW-846-3540 A,3620 A & 8080 
   
G. Finger Print Organic   ASTM D96 - 88 
(untuk contoh oil dalam padatan/ cairan)  
   
H. BTEX  (soil)  US EPA SW-846, 8260B 
   
I. PAH  (soil)  US EPA SW-846, 8270C 

 

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